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| 1 | Nonlinear characteristics analyses of particle motion for predicting flow regimes显示文摘Gas-solid flow regimes have a significant impact on particle transport and separation in a fluidized bed reactor.In this study,to determine flow regime transitions in gas-solid fluidized beds,an acoustic technique was used to detect and analyze the behavior of gas and solids.Algorithm complexity,fluctuation complexity,and Shannon entropy analyses of acoustic emission signals were performed to examine non linear system characteristics,and to determine the flow regime transiti on velocities uc,uk,and ufd-Moreover,using the standard deviation of pressure signals,pressure measurements and acoustic measurements were compared.The relative deviations(RDs)between the experimental and empirical values of uk were 8.8%,13.7%,8.8%,and 30.4%for the algorithm complexity,fluctuation complexity,Shannon entropy,and pressure signal standard deviation,respectively,while the respective RDs for Ufd were 15.7%,23.9%,15.7%,and 97.8%.The RDs between the experimental and empirical values of uc were all 6.4%.The experimental values obtained from acoustic signal measurements were therefore closer to the empirical values.In summary,the integration of non-intrusive acoustic measurements,complexity analysis,and Shannon entropy analysis is suitable for identifying flow regime transitions. | Panxing Kang Yujian Lu Lei Yang Libin Liu Xiayi(Eric)Hu Xiao Luo Hongbo Chen Yefeng Zhou Rui Zhang | 2020 | Particuology2020，18，6： | 1 |
| 2 | Synthesis of highly-branched Au@AgPd core/shell nanoflowers for in situ SERS monitoring of catalytic reactions显示文摘Alloy and small size nanostructure s are favorable to catalytical performance,but not to surface-enhanced Raman spectroscopy(SERS) applications.Integrating SERS and catalytic activity into the nanocrystals with both alloy and small size structures is of great interest in fabrication of SERS platform to in situ monitor catalytical reaction.Herein,we report a facile method to synthesize Au@AgPd trimetallic nanoflowers(Au@AgPd NFs) with both SERS and catalytic activities,through simultaneous selective growth of Ag and Pd on Au core to form highly-branched alloy shell.These nanocrystals have the properties of small sizes,defects abundance,and highly-dispersed alloy shell which offer superior catalytic activity,while the merits of monodisperse,excellent stability,and highly-branched shell and core/alloy-shell structure promise the enhanced SERS activity.We further studied their growth mechanisms,and found that the ratio of Ag to Pd,sizes of Au core,and surfactant cetyltrimethylammonium bromide together determine this special structure.Using this as-synthesized nanocrystals,a monolayer bifunctional platform with both SERS and catalytical activity was fabricated through selfassembly at air/water interface,and applied to in situ SERS monitoring the reaction process of Pdcatalyzed hydrogenation of 4-nitrothiophenol to 4-aminothio p henol. | Yujian Lai Lijie Dong Rui Liu Shaoyu Lu Zuoliang He Wanyu Shan Fanglan Geng Yaqi Cai Jingfu Liu | 2020 | Chinese Chemical Letters2020，31，9： | 0 |
| 3 | Topology optimization design of the main structure of 6-DOF manipulator based on the variable density method显示文摘In order to solve the problems of too large mass,too complex structure and poor flexibility of the 6 DOF manipulator,the topological optimization theory based on variable density method is applied to the 6-DOF manipulator,the topology optimization of the main structural components of the manipulator is carried out with the help of the finite element software ANSYS,and the optimized structure is simplified according to the density distribution of the units and the requirements of manufacturability.the results are compared and analysed by static mechanics.It shows that the whole mass of the 6-DOF manipulator is reduced by 47.23%without changing the original mechanical properties after topological optimization,and the optimized model can meet the requirements of manufacturability,the optimization effect is signifcant,which can be used as a reference for the structure optimization of the 6-DOF manipulator. | Yujian RUI Yongming LIU Zhen ZHANG Zhijian TU Jian WU Neng WEI Zhuanzhe ZHAO | 2022 | Mechanical Engineering Science2022，4，1： | 0 |
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