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| 1 | 湿气条件下的管道腐蚀显示文摘在压力小于 1 82MPa、温度为 4 0℃时 ,测量了 10cm管径高压管道顶部和底部的二氧化碳(CO2 )湿气腐蚀速率。在气体流速小于 11m s和液体流速小于 0 2m s时 ,测定其流型。介质为去离子水和CO2 气体。在试验条件下的流型为环型或接近层状环流过渡区。在 3h后腐蚀速率趋于稳定且随气体流速、液体流速和CO2 分压的增加而增长。试验结果可应用于油田条件。 | Y.H.Sun 郑君 黄红兵 | 2002 | 国外油田工程2002,18,8: | 6 |
| 2 | Microstructure change in Fe-based metallic glass and nanocrystalline alloy induced by liquid nitrogen treatment显示文摘The effects of acyclic liquid nitrogen(LN)treatment in a temperature range of-196℃to 50℃on the thermal and magnetic stability of Fe78Si9B13 and Fe73.5Si13.5B9Nb3Cu1 glassy ribbons have been studied.The intrinsic heterogeneities of the metallic glasses can be activated through cryogenic thermal cycling,making irreversible structural changes after the treatment and inducing rejuvenation to the materials.The microstructural changes of both Fe-based metallic glass(MG)and nanocrystalline alloy induced by LN treatment were investigated.The experimental results show that the LN treatment could effectively rejuvenate the Fe-Si-B MGs and change their thermomechanical and magnetic properties.Based on the partially-crystallinity and well-known magnetic constants,the increase of the energy at the order of 10m J/g and magnetic domain wall movement and rotation at the order of 5-6μm and 0.5°-0.8°are found for FINEMET-type amorphous alloy after LN treatment.It is also found that LN treatment can contribute a little stored energy to the magnetic domain wall movement and magnetic domain rotation. | M.C.Ri D.W.Ding Y.H.Sun W.H.Wang | 2021 | Journal of Materials Science & Technology2021,,10: | 3 |
| 3 | Rotational and translational domains of beta precipitate in aged binary Mg-Ce alloys显示文摘The structural evolution fromβ_(1)(Mg_(3)Ce)toβ(Mg_(12)Ce)precipitates,which takes place at the over-aged stage of binary Mg-Ce alloys,are investigated by high-angle annular dark-field scanning transmission electron microscopy.The structural transformation mainly occurs in the{111}_(β1)crystallographic planes,where the newly formedβlattices exhibit two categories of domain structures,namely rotational and translational domains.The rotational domain is composed of threeβdomains(β_(RA),β_(RB)andβ_(RC)),which are related by a 120°rotation with respect to each other around the 111_(β1)axis of theirβ_(1)parent phase.The{111}_(β1)crystallographic planes can provide four sets of sublattices with the same orientation for an initial nucleation ofβlattice.It leads to the formation of four translationalβdomains(β_(TA),β_(TB),β_(TC)andβ_(TD)),among which any two differ by a vector of 1/6112_(β1).We deduce theoretically that there exist twenty-fourβdomains during this transition.However,considering the interfacial misfit,only one-third of domains can grow up and eventually formsβribbon.Furthermore,a majority ofβribbons overlap partiallyβ_(1)plate,which is beneficial to relax interfacial strain amongβ,β_(1)andα-Mg matrix(α/β/β_(1)).The configuration of multipleβdomains can effectively regulate interfacial misfit ofα/βandβ/β_(1),which are responsible for enhancing the hardness and strength of Mg-Ce alloy.Additionally,this study aims to provide some clues to improve the over-aged performance of magnesium alloys by constructingβdomains and optimizing theα/β/β_(1)interface. | B.Z.Sun H.X.Zhang Y.Dong J.X.Ren Y.Tian G.M.Xie J.Tan Y.H.Sun Na Xiao | 2021 | Journal of Magnesium and Alloys2021,9,3: | 2 |
| 4 | High permittivity and low loss dielectric ceramics in the BaO-La2O3-TiO2-Ta2O5 system显示文摘 | X.M.Chen Y.H.Sun X.H.Zheng | | 0,,23: | 1 |
| 5 | Composition and size dependent torsion fracture of metallic glasses显示文摘The fracture of metallic glasses(MGs)of different compositions and sizes down to micrometers under torsion loading were systematically investigated.Contrary to the flat shear fracture along the circumferential plane as commonly supposed under torsion,we find that the torsion fracture of metallic glasses can deviate from flat shear plane,and the fracture angle is closely dependent on the composition and the size of MG samples.With a conversion method,we show that the torsion fracture of both millimeterand micrometer-sized MGs can be described by the ellipse fracture criterion as originally proposed for the tension fracture.The deviation from the circumferential shear plane under torsion is further shown to intrinsically relate to the fracture toughness of MGs.The tougher MG tends to have a smaller fracture angle with respect to the maximum shear plane,and vice versa,indicating a correlation between the fracture toughness and pressure/normal stress sensitivity in MGs.Our results provide new insights on the fracture mechanism and are helpful to design and control the deformation and fracture behavior of MGs under torsion loading. | J.Dong J.Shen Y.H.Sun H.B.Ke B.A.Sun W.H.Wang H.Y.Bai | 2021 | Journal of Materials Science & Technology2021,,23: | 1 |
| 6 | A negative deviation from Porod’s law in SAXS of organo—MSU—X显示文摘Small-angle X-ray scattering(SAXS)using synchrotron radiation as X-ray source has been employed to charactcizc the microscopic structrure of organo-modified mesoporous molecular sieves(organo-MSU-X)prepared by a one-pot template-directed synthesis.It is shown that the SAXS profile is hardly constant with Porod’s law showing a negative slope,i.e.,negative deviation.This suggests that there is diffuse interfacial layer located between the pores and the matrix.This suggests that the organic groups remain covalently linked to the matrix,as indicated by ^29SiCP MAS NMR and FT-IR.The average thickness of the interfacial layer was found to be about 1nm for each of the three samples with different kinds and the same amounts(20? of organic groups.This kind of material has also been proved to possess both surface and mass fractal structure of the amophous porous silica materials.2001 Elsevier Science B.V.All rights reserved. | Z.H.Li Y.J.Gong D.Wu Y.H.Sun J.Wang Y.Liu B.Z.Dong Y.J. | 2001 | Beijing Synchrotron Radiation Facility2001,,2: | 0 |