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| 1 | 高效液相色谱-紫外检测法同时测定药物制剂及人体血清中的奥美沙坦酯和厄贝沙坦及氢氯噻嗪(英文)显示文摘A simple,selective,sensitive,precise,simultaneous high performance liquid chromatographic analysis of serum samples and commercial tablet formulation containing hydrochlorothiazide,olmesartan medoxomil and irbesartan are reported.Good chromatographic separation was achieved using a μ-Bondapak,C18 column(15 cm×4.6 mm,5 μm),and a mobile phase consisting of acetonitrile-0.2% acetic acid aqueous solution(50∶50,v/v)at a flow rate of 1.0 mL/min.The ultraviolet detector was set at a wavelength of 260 nm.Hydrochlorothiazide,olmesartan medoxomil,and irbesartan were eluted at 1.2,3.8,and 4.4 min,respectively.No extraneous materials were found to interfere.The method uses protein precipitation with acetonitrile for the preparation of serum sample.The linear ranges for hydrochlorothiazide,olmesartan medoxomil,and irbesartan were 6.25-18.75,20-60,and 75-225 ng/mL,respectively.The recoveries of hydrochlorothiazide,olmesartan medoxomil,and irbesartan in spiked samples were all greater than 98%,and their relative standard deviations were less than 2.0%.The limits of detection were 1,2,and 2 ng/mL for hydrochlorothiazide,olmesartan medoxomil,and irbesartan,respectively,and the limits of quantification were 3 ng/mL,which allow their determination at the expected serum concentration levels. | SULTANA Najma ARAYNE M Saeed ALI S Shahid SAJID Shahnawaz | 2008 | 色谱2008，26，5： | 6 |
| 2 | Unsteady flow of a second grade fluid film over an unsteady stretching sheet显示文摘 | Abbas Z Hayat T Sajid M | 2008 | Math Computer Modelling2008，48，34： | 1 |
| 3 | Analytic solution for MHD rotating flow of a second grade fluid over a shrinking surface显示文摘 | Hayat T Javed T Sajid M | 2008 | Phy Lett A2008，372，18： | 1 |
| 4 | MHD stagnation-point flow of an upper-convected Maxwell fluid over a stretching surface显示文摘 | Hayat T Abbas Z Sajid M | 2009 | Chaos Solitons and Fractals2009，39，2： | 1 |
| 5 | Endovascular aortic aneurysm repair (EVAR)has significantly lower perioperative mortality in comparison to open repair:a systematic review显示文摘 | Sajid MS Desai M Haider Z | 2008 | Asian J Surg2008，31，3： | 1 |
| 6 | The role of alpha(v) beta3 integrins in vascular healing显示文摘 | Sajid M Stouffer G A | 2002 | Thromb Haemost2002，87，2： | 1 |
| 7 | Alphavbeta3-integrin antagonists inhibit thrombin-induced proliferation and focal adhesion formation in smooth muscle cells显示文摘 | Sajid M Zhao R Pathak A | 2003 | Am J Physiol Cell Physiol2003，285，5： | 1 |
| 8 | Deposition of Phosphate Nanoparticles onto Textile Fabrics via Sol-gel Method and Their Kinetics Desorption Studies显示文摘In this paper,phosphate nanoparticles were coated on cotton(CO)and polyester(PES)textile surfaces by sol-gel method using tetraethylorthosilicate(TEOS)and chloropropyltriethoxysilane(CPTS)as silica precursors.The deposited nanoparticles were observed with scanning electronic microscopy energv-dispersive X-ray spectroscopy(SEM-EDX).The release kinetics of phosphorus(P)from these textiles into the aqueous medium(Aq),acid(Ac),and basic(Ba)artificial sweats were then studied.The released amount of phosphorus was evaluated by the inductively coupled plasma(ICP)according to ISO NF EN 16711-2 procedure.The results revealed that the release of P into the aqueous medium is lower than in the artificial sweat.The kinetics data[the phosphoras desorption amount(mg/g)as a iunction of time]were modeled according to five models:the first order,the second order,the third order,simple Elovich and parabolic diffusion.The suitable model was chosen based on the coefficient of determination(R2)and the calculation of the sum of the absolute errors(EABS),which describes the error between the theoretical and experimental values.SEM observations were also carried out on the fabrics after desorption in order to show the impact of desorption on their morphology.Furthermore,the impact of P release on the tensile strength of CO and PES fabrics was investigated using a uniaxial tensile test.The thennal stability of all samples before and after desorption was assessed by thermogravimetric aiialysis(ATG). | Mohamed El MESSOUDI Aicha BOUKHRISS Laila SADALLAH Laila SAJID M'hamed El KOUALI Said GMOUH | 2020 | Chemical Research in Chinese Universities2020，36，5： | 1 |
| 9 | Cysteine proteases of parasitic organisms 显示文摘 | Sajid M McKerrow JH | 2002 | Mol Biochem Parasitol2002，120，： | 1 |
| 10 | Homotopy analysis of MHD boundary layer flow of an upper-convected Maxwell fluid显示文摘 | Hayat T Sajid M | 2007 | Int J Eng Sci2007，45，28： | 1 |
| 11 | Immunomodulatory effect of various anti-parasitics:a review显示文摘 | SAJID M S IQBAL Z MUHAMMAD G | 2006 | Parasitology2006，132，3： | 1 |
| 12 | Upper limb deep vein thrombosis:a literature review to streamline the protocol for management显示文摘 | Sajid MS Ahmed N Desai M | 2007 | Acta Haematol2007，118，： | 1 |
| 13 | Differential effects of cadmium and chromium on growth,photosynthetic activity,and metal uptake of Linum usitatissimum in association with Glomus intraradices显示文摘 | AMNA C NAEEM A SAJID M | 2015 | Environ Monit Assess2015，187，： | 1 |
| 14 | Evolution of apoptosis-like programmed cell death in unicellular protozoanparasites 显示文摘 | Kaczanowski S Sajid M Reece S E | 2011 | Parasites & Vectors2011，4，4： | 1 |
| 15 | Drugs targeting parasite lysosomes显示文摘 | Doyle PS Sajid M O'Brien T | 2008 | Curt Pharm Des2008，14，9： | 1 |
| 16 | Systematic review and meta-anal- ysis of the use of lightweight versus heavyweight mesh in open inguinal her- nia repair 显示文摘 | SAJID M S LEAVER C BAIG M K | 2012 | British Journal of Surgery2012，99，1： | 1 |
| 17 | Knee length ver- sus thigh length graduated compression stockings for prevention of deep vein thrombosis in postoperative surgical patients显示文摘 | Sajid MS Desai M Morris RW | 2012 | Cochrane Database Syst Rev2012，5，00： | 1 |
| 18 | Detecting pediatric autoimmune neuropsychiatric disorders with straptococcus in children with obsessive-compulsive disorder and tics 显示文摘 | Murphy TK Sajid M Sota O | 2004 | Biol Psychiatry2004，55，： | 1 |
| 19 | Comparative studies on molecular changes and pro-oxidative activity of haemoglobin from dif- ferent fish species as influenced by pH显示文摘 | Sajid M Soottawat B | 2011 | Food Chemistry2011，124，3： | 1 |
| 20 | Design and implementation of a face recognition system using Fast PCA显示文摘 | SAJID I AHMED M M TAJ I | 2008 | IEEE Translation on Computer Society2008，16，8： | 1 |
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