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		题名	作者	年代	出处	被引量
	1	Simultaneous determination of amlodipine,valsartan and hydrochlorothiazide by LC-ESIMS/MS and its application to pharmacokinetics in rats显示文摘Polypill is a fixed-dose combination that contains three or more active ingredients used as a single daily pill to achieve a large effect in preventing cardiovascular disease with minimal adverse effects.A novel and accurate liquid chromatography tandem mass spectrometry method using electrospray ionization mode has been developed and validated for the simultaneous determination of amlodipine(AMD),valsartan(VAL) using losartan(LOS) as an internal standard(IS),and hydrochlorothiazide(HCT) using furosemide(FSD) as an IS.The separation was carried on Aquasil C_(18)(50 mm×2.1 mm,5μm) reversed phase column using acetonitrile and water containing 0.1%formic acid(50:50,v/v) as the mobile phase.The method was validated in terms of linearity,accuracy and precision over the concentration range of 1-1000 ng/mL.The intra and inter-day precision and accuracy,stability and extraction recoveries of all the analytes were in the acceptable range.This method can be successfully applied to the pharmacokinetic study of AMD,VAL and HCT when given as a polypill.	Shankar Ganesh Gadepalli Pragney Deme Madhusudana Kuncha Ramakrishna Sistla	2014	Journal of Pharmaceutical Analysis2014，4，6：	5
	2	An improved dis- persive solid-phase extraction clean-up method for the gas chromatog- raphy-negative chemical ionisation tandem mass spectrometric deter- mination of multiclass pesticide residues in edible oils显示文摘	Pragney Deme Tirupathi Azmeera Devi B L A	2014	Food Chem- istry2014，142，1：	1
	3	An improved dispersive solid - phase extraction clean - upmethod for the gas chromatography - negative chemical ionisationtandem mass spectrometric determination of multiclass pesticideresidues in edible oils 显示文摘	Pragney Deme Tirupathi Azmeera B L A Prabhavathi Devi	2014	Food Chemistry2014，142，：	1

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