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| 1 | 程序升温汽化大体积进样气相色谱法同时测定空气中的甲醛及其他10种羰基污染物(英文)显示文摘Long-term indoor-air limit for formaldehyde stipulated by the European Commission is 1 μg/m3,while the World Health Organization has set a threshold of 100 μg/m3 that should not be exceeded for more than 30 min. To date,however,only a few analytical techniques have been developed that can be used to detect formaldehyde at these very restrictive limits. Thus,there is a need to develop for comprehensive methods for analyzing airborne formaldehyde and other carbonyl pollutants in the ambient environment. The aim of this study is to develop a highly sensitive online automated preconcentration gas chromatographic method using large-volume injection with a programmed temperature vaporization injector for the analysis of airborne formaldehyde and ten other carbonyl compounds. The influence of several parameters,such as the maximum volume injected,programmed temperature vaporization transfer time and temperature,carrier gas flow rate,and type of packing material was investigated. After optimization,highly satisfactory results in terms of the absolute and methodological detection limits were achieved,i. e. as low as the μg/m3 level for all the carbonyl pollutants studied. A commercially available sampler,originally designed for active sampling,was evaluated as a passive sampling device;this optimized technique was applied to monitor the concentrations of carbonyl pollutants in the indoor air of ten public buildings in Florence. The strength of this methodology lies both in the low detection limits reached in the simultaneous analysis of a wide group of 2,4-dinitrophenylhydrazine derivatives,and the potential adaptability of this method to other gas chromatographic applications to achieve lower sensitivity. | Stefano DUGHERI Nicola MUCCI Ilenia POMPILIO Giovanni CAPPELLI Costanza BOSSI AlessANDro BONARI Giulio ARCANGELI | 2018 | 色谱2018，36，12： | 3 |
| 2 | 生活方式和饮食因素:预防致死性前列腺癌显示文摘预防致死性前列腺癌是一个重要的公共卫生难题。解决该难题可以改善人们的健康状况,减少罹患该疾病的痛苦。本综述围绕某些与致命性前列腺癌预防有关的生活方式和饮食因素研究进行讨论。我们还对以下行为风险因素的研究进行总结:肥胖和体重变化、体育活动、吸烟状况、抗氧化剂摄入量、维生素D和钙、以及咖啡摄入量。 | Kathryn M Wilson Edward L Giovannucci Lorelei A Mucci | 2012 | Asian Journal of Andrology2012，14，3： | 3 |
| 3 | A 3-year naturalistic study of 53 preschool children with pervasive developmental disorders treated with risperidone显示文摘 | Masi G Cosenza A Mucci M | 2003 | J Clin Psychiatry2003，64，： | 1 |
| 4 | Neuroendocrine expression in metastatic prostate cancer:evaluation of high throughput tissue microarrays to detect heterogeneous protein expression 显示文摘 | Akdas G Manely S | 2000 | Hum Pathol2000，31，4： | 1 |
| 5 | 1H and 13C nuclear magnetic resonance identification and characterization of components of chondroitin sulfates of various origin 显示文摘 | Mucci A Schenetti L Volpi N | 2000 | Carbohydrate Polymers2000，41，1： | 1 |
| 6 | Hemorrhagic corpusluteum cysts : An unusual problem for pediatric surgeons显示文摘 | Pinelli C Giacomo MD Mucci N | 2009 | J Pediatr Ado- lesc Gyneco12009，22，： | 1 |
| 7 | A novel approach to digital beamforming显示文摘 | Roger G Pridham Ronald A Mucci | 1978 | J Acoust Soc Am1978，63，2： | 1 |
| 8 | Prospective study of prostate tumor angiogenesis and cancer-specific mortality in the health professionals follow-up study显示文摘 | Mucci LA Powolny A Giovannucci E | 2009 | J Clin Oncol2009，27，33： | 1 |
| 9 | Oxygen isotope fractionation between synthetic aragonite and water: Influence of temperature and Mg2 concentration 显示文摘 | KIM S T O' NEIL J R HILLAIRE-MARCEL C MUCCI A | 2007 | Geochimica Et Cosmochimica Acta2007，71，19： | 1 |
| 10 | Symptomatology and comorbidity of generalized anxiety disorder in children and adolescents显示文摘 | Masi G Mucci M Favilla L | 1999 | Compr Psychiatry1999，40，： | 1 |
| 11 | Perceptions of genetically modified foods by consumers in Argentina 显示文摘 | Andrea Mucci Guillermo Hough | 2003 | Food Quality and Preference2003，15，： | 1 |
| 12 | Calcite precipitation in seawater using a constant addition technique: A new overall reaction kinetic expression 显示文摘 | Zhong Shaojun Mucci A | 1993 | Geochimica et CosmochimicaActa1993，57，7： | 1 |
| 13 | Age at menarche and age at menopause in relation to hepatoeellular carcinoma in women 显示文摘 | Mucci LA Kuper HE Tamimi R | | BJOG0，108，3： | 1 |
| 14 | A review of the biochemistry of heavy metal biosorption by brown algae显示文摘 | DAVIS T A VOLESKY B MUCCI A | 2003 | Water Research2003，37，： | 1 |
| 15 | Partitioning of rare earth elements (REEs) between calcite and seawater solutions at 25 °C and latin, and high dis- solved REE concentrations 显示文摘 | Zhong S Mucci A | 1995 | Geochimica et Cosmoehimiea Aeta1995，59，3： | 1 |
| 16 | A review of the biochemistry of heavy metal biosorption by brown algae显示文摘 | DAVIS T A VOLESKY B MUCCI A | 2003 | Water Research2003，37，43： | 1 |
| 17 | A 25-year prospective study of plasma adiponectin and leptin concentrations and prostate cancerrisk and survival 显示文摘 | Li H Stampfer M J Mucci L | 2010 | Clin Chem2010，56，： | 1 |
| 18 | A prospective study on dietary acrylamide intake and the risk for breast,endometrial,and ovarian cancers显示文摘 | WILSON K M MUCCI L A ROSNER B A | 2010 | Cancer Epidemiology Biomarkers Prevention2010，19，10： | 1 |
| 19 | Growth kinetics and composition of magnesian calcite overgrowths precipitated from seawater: Quantitative influence of orthophosphate ions 显示文摘 | Mucci A | 1986 | Geochimica et Cosmochimica Acta1986，50，10： | 1 |
| 20 | Dorsolateral pre-frontal cortex volume in patients with deficit or nondeficitschizophrenia显示文摘 | Volpe U Mucci A Quarantelli M | 2012 | Prog Neuropsychopharmacol Biol Psychia-try2012，37，： | 1 |
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