| 1 | Synthesis and Characterization of Mesoporous Alumina via a Reverse Precipitation Method显示文摘Mesoporous alumina γ-Al_2O_3 with high specific surface area and large pore volume is prepared by using a facile reverse precipitation method from sodium aluminate and nitric acid.The effects of terminal pH value,aging time and thermal stability on the characterization of γ-Al_2O_3 are studied by means of X-ray diffraction(XRD),Fourier transform infrared spectroscopy(FTIR),Brunauer-Emmett-Teller(BET) method and scanning electron microscopy(SEM).The results show that γ-Al_2O_3 with better properties can be obtained by changing the preparation parameters.High BET surface area of 340(m^2)/g can be obtained by calcining at 500 ℃ for 4 h with large pore volume of 0.90(cm)~3/g and average pore size of 7.6 nm.After calcining at 1000°,the surface area is still 86 m2/g and the pore volume is 0.37(cm)~3/g. | Y.S.Wu J.Ma F.Hu M.C.Li | 2012 | Journal of Materials Science & Technology2012，28，6： | 3 |
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