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1Tensile strength and damage of open-cell ceramic foams under cylindrical splitting test显示文摘To widen the understanding of tensile failure of reticulated ceramic foams and expand the available mechanical method,a cylindrical splitting test is developed in the present study based on alumina open-cell foams of three different pore densities.The biaxial method is validated by characterization of mechanical parameters,and the in-situ fracture process is validated by a digital image correlation,followed by a formula correction for effective tensile strength with consideration of discrete crack paths.For experimental setup curved loading platens,compliant pad and intermediate quasi-static loading rate are proposed for guaranteeing tensile failure under a radial compressive load.Tensile strength,fracture energy,and brittleness increase with the foam pore density,and the fracture behavior is a balanced result of materials and foam structural support strength.An analytical model of splitting tensile strength with structural parameters is derived,which implies its dependence on cell size and critical stress intensity factor of strut materials.Yajie Dai Jana Hubálková Claudia Voigt Martin Abendroth Xiong Liang Wen Yan Yawei Li Christos G.Aneziris 2023Journal of Advanced Ceramics2023,12,11:0
2Efficient fabrication of light Cf/SiHfBOC composites with excellent thermal shock resistance and ultra-high-temperature ablation up to 1800℃显示文摘In this paper,a high-yield Hf-modified SiHfBOC ceramic precursor was developed,and a high-pressure assisted impregnation pyrolysis method was proposed to achieve the preparation of 3D PyC–Cf/SiHfBOC composites.This high-pressure assisted impregnation method significantly improves impregnation filling effect of the precursor in and between fiber bundles compared to dozens of traditional impregnation cycles.After undergoing just 9 precursor infiltration pyrolysis(PIP)cycles,the composites achieved relative density of approximately 90%and density of 1.64 g/cm^(3).The critical temperature difference of the 3D PyC–Cf/SiHfBOC composites after the shock of room temperature(RT)–1000℃is as high as 650℃,which is twice that of traditional ceramic materials,showing good thermal shock resistance.Under the effect of Hf modification,a dense HfO_(2)–SiO_(2)oxide layer(thickness of 93μm)was formed in situ on the surface of the 3D PyC–Cf/SiHfBOC composites,effectively preventing further erosion of the composite matrix by high-temperature oxidation gas.Even in the ultra-high-temperature oxygen-containing environment at 1800℃,it still exhibits an excellent non-ablative result(with a linear ablation rate of 0.83×10^(−4)mm/s).This work not only enriches the basic research on lightweight ultra-high-temperature ceramic composites converted from Hf ceramic precursors,but also provides strong technical support for their applications in ultra-high-temperature non-ablative thermal protection materials for high-speed aircraft.Yang Lyu Zhihong Han Guangdong Zhao Yuan Cheng Shanbao Zhou Xinghong Zhang Guiqing Chen Wenbo Han 2023Journal of Advanced Ceramics2023,12,11:0
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