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| 1 | Double diamond structured bicontinuous mesoporous titania templated by a block copolymer for anode material of lithium-ion battery显示文摘Titania has received considerable attention as a promising anode material of Li-ion battery(LIB).Controlling the structure and morphology of titania nanostructures is crucial to govern their performance.Herein,we report a mesoporous titania scaffold with a bicontinuous shifted double diamond(SDD)structure for anode material of LIB.The titania scaffold was synthesized by the cooperative self-assembly of a block copolymer poly(ethylene oxide)-block-polystyrene template and titanium diisopropoxide bis(acetylacetonate)as the inorganic precursor in a mixture solvent of tetrahydrofuran and HCl/water.The structure shows tetragonal symmetry(space group I4_(1)/amd)comprising two sets of diamond networks adjoining each other with the unit cell parameter of a=90 nm and c=127 nm,which affords the porous titania a specific surface area(SSA)of 42 m^(2)·g^(-1)with a mean pore diameter of 38 nm.Serving as an anode material of LIB,the bicontinuous titania scaffold exhibits a high specific capacity of 254 mAh·g^(-1)at the current density of 1 A·g^(-1)and an alluring self-improving feature upon charge/discharge over 1,000 cycles.This study overcomes the difficulty in building up ordered bicontinuous functional materials and demonstrates their potential in energy storage application. | Qingqing Sheng Qian Li Luoxing Xiang Tao Huang Yiyong Mai Lu Han | 2021 | Nano Research2021，14，4： | 2 |
| 2 | Free-standing hybrid films comprising of ultra-dispersed titania nanocrystals and hierarchical conductive network for excellent high rate performance of lithium storage显示文摘The construction of advanced electrode materials is key to the field of energy storage.Herein,a free-standing anatase titania(TiO_(2))nanocrystal/carbon nanotube(CNT)film is reported using a simple and scalable sol-gel method,followed by calcination.This unique free-standing film comprises ultra-small TiO_(2) nanocrystals(~5.9 nm)and super-aligned CNTs,with ultra-dispersed TiO_(2) nanocrystals on the surfaces of the CNTs.On the one hand,these TiO_(2) nanocrystals can significantly decrease the diffusion distance of the charges and on the other hand,the cross-linked CNTs can act as a three-dimensional(3D)conductive network,allowing the fast transport of electrons.In addition,the film is free-standing,without requiring electrode fabrication and additional conductive agents and binders.Owing to these above synergistic effects,the film is directly used as an anode in Li-ion batteries,and delivers a high discharge capacity of~105 mAh·g^(−1) at high rate of 60 C(1 C=170 mA·g^(−1))and excellent cycling performance over 2,500 cycles at 30 C.These results indicate that the free-standing anatase TiO_(2) nanocrystal/CNT film affords a superior performance among the various TiO_(2) materials and can be a promising anode material for fast-charging Li-ion batteries.Moreover,the TiO_(2)/CNT film exhibits an areal capacity of up to 2.4 mAh·cm^(−2),confirming the possibility of its practical use. | Kunlei Zhu Chenyu Li Yushuang Jiao Jiawen Zhu Hongtao Ren Yufeng Luo Shoushan Fan Kai Liu | 2021 | Nano Research2021，14，7： | 1 |
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