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| 1 | Synthesis, Crystal Structure and Anti-TMV Activity of(Z)-4-[3-(4-Methyl-1,2,3-thiadiazol-5-yl)-3-(4-trifluoromethylphenyl)acryloyl]morpholine显示文摘The target compound(Z)-4-[3-(4-methyl-1,2,3-thiadiazol-5-yl)-3-(4-trifluoromethylphenyl)acryloyl]morpholine was synthesized by the nucleophilic substitution,Horner-Emmons reaction,ester hydrolysis,and condensation.Its structure was characterized by NMR,H RMS and single-crystal X-ray diffraction.The crystal of the target compound belongs to monoclinic system,space group P2_(1) with a=11.5058(15),b=6.6626(10),c=23.184(3)Å,V=1777.3(4)Å^(3),Z=8,D_(c)=1.496 Mg/m^(3),F(000)=792 andμ=0.229 mm^(–1).X-ray analysis indicated C–H....O intermolecular H-bonds in this crystal structure.The target compound exhibited 53%curative activity against TMV. | 孙素素 李晴 高卫 李晓天 陈来 张金林 | 2021 | Chinese Journal of Structural Chemistry2021，40，1： | 1 |
| 2 | 杨宣舒主任医师治疗胃下垂的经验显示文摘 | 岳良明 | 2000 | 四川中医2000，18，3： | 0 |
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