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| 1 | 3,3’-(3-氟基苯亚甲基)双(吲哚-2-甲酸甲酯)的合成及其晶体结构显示文摘以吲哚-2-甲酸甲酯和对氟基苯甲醛为原料,在微波辐射条件下,以CuBr2为催化剂,成功合成了一种双吲哚甲烷类化合物3,3'-(3-氟基苯亚甲基)双(吲哚-2-甲酸甲酯)(3),产物结构经1H NMR、13C NMR、ESI-MS、FT-IR、元素分析及X-单晶衍射表征。产物(3)属三斜晶系,P-1空间群,晶胞参数ɑ=9.6770(19)A,b=10.111(2)A,c=12.818(3)A,β=82.77(3)°,V=1132.3(5)A^3,Z=2,F(000)=2332,μ=0.10 mm^-1,R[F^2>2σ(F2)]=0.068,wR(F2)=0.191[I>2σ(I)]。 | 施星浩 周进 凌天 张志远 李玉龙 蒋蕻 孙宏顺 | 2019 | 安徽化工2019，45，6： | 0 |
| 2 | Synthesis,characterization and antibacterial screening of some novel 1,2,4-triazine derivatives显示文摘A new series of 1, 2, 4-triazine derivatives possessing indole nucleus were synthesized with an aim to explore their effect on in vitro growth of microorganisms causing microbial infection. In vitro antimicrobial activity was performed against S. aureus, S. epidermidis, P. mirabilis and E. coli using disk diffusion method. The MIC was detected using the double dilution method. The results were compared by calculating percent inhibition area/mg of the compounds with the standard drug 'Ciprofloxacin'.Selected compounds were evaluated for toxic effects using human hepatocellular carcinoma(HepG2) cell line by MTT-assay. Results revealed that some compounds of the series were found to exhibit better activity with less toxicity than | Mohammad Arshad Abdul Roouf Bhat Kwon Kang Hoi Inho Choi Fareeda Athar | 2017 | Chinese Chemical Letters2017，28，7： | 0 |
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