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| 1 | 注浆成型法制备氧化钇稳定的氧化锆透氧膜及其性能显示文摘采用注浆成型法制备8%(摩尔分数)氧化钇稳定氧化锆(8YSZ)透氧膜,分析浆料特性、烧结特性和电学性能并将其用于固体透氧膜(SOM)法制备金属。结果表明:当添加4%(质量分数)柠檬酸作为8YSZ浆料分散剂时,浆料相对黏度为1.82,Zeta电位为–43.7mV。透氧膜素坯经1 700℃煅烧2 h后,物相全部转化为立方相,相对密度达到99.1%。在500℃时,1 700℃烧结成型的透氧膜总电阻最小,为149.38Ω,总电导率最大,为5.84×10–4 S/cm。该法制备的膜管经SOM法电解脱氧实验证明具有优良的控氧性能和抗熔盐侵蚀特性。 | 沈斌 邹星礼 程红伟 赖冠全 鲁雄刚 | 2015 | 硅酸盐学报2015，43，6： | 3 |
| 2 | Environmental and energy gains from using molten magnesium–sodium–potassium chlorides for electro-metallisation of refractory metal oxides显示文摘The molten eutectic mixture of magnesium,sodium and potassium chlorides(Mg Cl2–Na Cl–KCl) has inappreciable solubility for oxide ions,and can help disengage a carbon anode from the oxide ions generated at a metal oxide cathode,and effectively avoid carbon dioxide formation.This 'disengaging strategy' was successfully demonstrated in electro-reduction of solid oxides of zirconium and tantalum.It has led to significantly higher current efficiency(93%),and lower energy consumption(1.4 k W h kg 1) in electrolysis of tantalum oxide to tantalum metal compared to the conventional electrolysis in molten calcium chloride(e.g.78% and 2.4 k W h/kg-Ta). | Wei Li Yating Yuan Xianbo Jin Hualin Chen George Z.Chen | 2015 | Progress in Natural Science:Materials International2015，25，6： | 2 |
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